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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2414780Generated: October 30, 2026

Morpholine → HCID 22643409, compound

https://huagongshe.com/reaction/2414780

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMorpholineHCID 8083—
ReactantHCID 22643414HCID 22643414—
ProductHCID 22643409HCID 2264340957.6%

Reaction Steps

0.56 g of ethyl 4-(2-benzimidazolylthio)valerate and 0.53 g of morpholine were heated at 100° C. for 20 hours. The reaction mixture was applied without treatment to a silica gel column for purification (methanol:methylene chloride=1:10), and 0.37 g of the title compound was obtained as solid (yield: 58%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06815455B1
Source datasetuspto-grants-2004_11
ORD IDord-dd7fd86d26374cfda598d7f403a59eef
Source noteuspto-grants-2004_11