HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 22643409, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 22643414 | HCID 22643414 | — |
| Product | HCID 22643409 | HCID 22643409 | 57.6% |
Reaction Steps
0.56 g of ethyl 4-(2-benzimidazolylthio)valerate and 0.53 g of morpholine were heated at 100° C. for 20 hours. The reaction mixture was applied without treatment to a silica gel column for purification (methanol:methylene chloride=1:10), and 0.37 g of the title compound was obtained as solid (yield: 58%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06815455B1 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-dd7fd86d26374cfda598d7f403a59eef |
| Source note | uspto-grants-2004_11 |