HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22640158, compound → 1-Biphenyl-4-yl-piperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22640158 | HCID 22640158 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Biphenyl-4-yl-piperazine | HCID 2735513 | — |
Reaction Steps
A suspension of 12.45 g (0.037 mol) of 1-benzyl-4-biphenyl-4-yl-piperazine and 4 g of palladium hydroxide in 360 ml of methanol is stirred for 6 hours at ambient temperature in a Parr apparatus under a hydrogen pressure of 50 psi. The catalyst is separated off and the filtrate is evaporated down.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818644B1 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-59a29e27e8a44363bf5f47598bfd299e |
| Source note | uspto-grants-2004_11 |