HuagongsheHuagongshe Chemistry Print Report · For research reference only
Heptane → HCID 22641070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Heptane | HCID 8900 | — |
| Reactant | HCID 22641097 | HCID 22641097 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 22641070 | HCID 22641070 | 36% |
Reaction Steps
In a manner similar to that of Example 7, by reaction of 600 mg (1.36 mmol) of ethyl 6-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylselanylethynyl)nicotinate in 30 ml of THF and 1 g of sodium hydroxide, and after trituration from heptane, 200 mg (36%) of the expected compound are obtained in the form of a yellow solid. m.p.=128° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818666B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-706341bbf6814894956a7622e176ad13 |
| Source note | uspto-grants-2004_11 |