HuagongsheHuagongshe Chemistry Print Report · For research reference only
Heptane → HCID 10224239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Heptane | HCID 8900 | — |
| Reactant | HCID 22641081 | HCID 22641081 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 10224239 | HCID 10224239 | 80.4% |
Reaction Steps
In a manner similar to that of Example 7, by reaction of 1.35 g (3.07 mmol) of methyl 4-(3,5,5,8,8-pentamethyl-5,6,7,8-tetrahydro-2-napthylselanylethynyl)benzoate in 20 ml of THF and 3 g of sodium hydroxide, and after trituration from heptane, 1.05 g (80%) of the expected compound are obtained in the form of a white solid. m.p.=240° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818666B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-8b20f9729af14381a065b2060118494d |
| Source note | uspto-grants-2004_11 |