HCID 22641069, compound → HCID 17886634, compound

HRID 2415246Notes

Reaction equation

HRID 2415246 reaction equation
[CH3:1][C:2]1([CH3:27])[CH2:11][CH2:10][C:9]([CH3:13])([CH3:12])[C:8]2[CH:7]=[C:6]([C:14]#[C:15][S:16][C:17]3[CH:26]=[CH:25][C:20]([C:21]([O:23]C)=[O:22])=[CH:19][CH:18]=3)[CH:5]=[CH:4][C:3]1=2>C1COCC1>[CH3:1][C:2]1([CH3:27])[CH2:11][CH2:10][C:9]([CH3:12])([CH3:13])[C:8]2[CH:7]=[C:6]([C:14]#[C:15][S:16][C:17]3[CH:18]=[CH:19][C:20]([C:21]([OH:23])=[O:22])=[CH:25][CH:26]=3)[CH:5]=[CH:4][C:3]1=2

Participants

3

Reactant 1

HCID 22641069HCID 22641069, compound

Product 1

HCID 17886634HCID 17886634, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

In a manner similar to that of Example 2, by reaction of methyl 4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylethynylsulphanyl)benzoate in THF, and after crystallization from heptane, the expected derivative is obtained in the form of white solid.

Workup

  1. customafter crystallization from heptane
  2. customthe expected derivative is obtained in the form of white solid

Sources & evidence

ORD record
ord-fdfb57507af64871a2cd3dd88011b9bc
Source dataset
uspto-grants-2004_11
Patent number
US06818666B2

Reaction notes

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