HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-1-ethenyl-2-fluorobenzene → 4-Bromo-1-ethyl-2-fluorobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-1-ethenyl-2-fluorobenzene | HCID 16660774 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-Bromo-1-ethyl-2-fluorobenzene | HCID 22641057 | — |
Reaction Steps
4-Bromo-2-fluoro-1-vinyl-benzene (1.80 g, 8.96 mmol) was dissolved in ethyl acetate (50 mL) and palladium-on-carbon (10%, 70 mg) was added and the mixture was hydrogenated under 1 atmosphere overnight. The mixture was filtered and the filtrate was concentrated to give the crude, 1.80 g, which was used directly for the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818663B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-59db2a2efae84a179b953dc86a8ba6c1 |
| Source note | uspto-grants-2004_11 |