HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 2-Bromo-1-(3-ethoxyphenyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | 1-(3-Ethoxyphenyl)ethanone | HCID 3770250 | — |
| Product | 2-Bromo-1-(3-ethoxyphenyl)ethanone | HCID 22641006 | — |
Reaction Steps
This compound was prepared from resin-bound thiourea of Example 24 and 2-bromo-(3-ethoxyphehyl)-ethanone by the procedure used in Example 36. MS (ES) MH+=453. The 2-bromo-(3-ethoxyphenyl)-ethanone was prepared by treating 1-(3-ethoxy-phenyl)-ethanone (prepared in accordance with the procedure in J. Chem. Soc. Perkin Trans. 2:1996, 755-760) with bromine as in Example 20C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818663B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-2a103c4c211c48989b7fa4bbd9802886 |
| Source note | uspto-grants-2004_11 |