HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10994934, compound → HCID 12993032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10994934 | HCID 10994934 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 12993032 | HCID 12993032 | — |
Reaction Steps
1,2,3,4-Tetrahydro-3-(3,4-methylenedioxyphenyl)-2-[(5-(4-nitrophenyl))-furoyl]-9H-pyrrolo[3,4-b]quinolin-9-one (25 mg, 0.0479 mmol) (prepared as in Example 33) was stirred with 10% Pd on Carbon (5.1 mg, 0.00479 mmol) under 1 atm H2 at room temperature for 14 h. The solvent was evaporated and product isolated by preparative TLC as a yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818646B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-688bd89bc7df49ddaf514346d7fe9ac7 |
| Source note | uspto-grants-2004_11 |