HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 22641899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22641896 | HCID 22641896 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22641899 | HCID 22641899 | 98.1% |
Reaction Steps
As described for example 43, the title compound (1.86 g, 98%) was prepared from a mixture of 6-(4-fluoro-benzyloxy)-3,4-dihydro-2H-isoquinolin-1-one (2 g, 7.37 mmol) and lithium aluminum hydride (0.559 g, 14.74 mmol) in tetrahydrofuran. MS: m/e=258.0 (M+H+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818774B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-c1764dbad2244da4b227bf838c98eed9 |
| Source note | uspto-grants-2004_11 |