HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 10473439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 69036512 | HCID 69036512 | — |
| Catalyst | Bis(triphenylphosphine)palladium | HCID 10122028 | — |
| Product | HCID 10473439 | HCID 10473439 | 25% |
Reaction Steps
As described for example 20f, the title compound (10 mg, 25%) was prepared from a mixture of 2-(R)-{2-[5-(4-Fluoro-benzyloxy)-2-iodo-phenyl]-acetylamino}-propionamide (50 mg, 0.109 mmol), triethylamine (0.030 mL, 0.218 mmol), bis (triphenylphosphine) palladium II chloride (1.5 mg, 0.0022 mmol) in 1 mL ethyl acetate. MS: m/e=357.2 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06818774B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-65544c9976a445d892f80542377efe56 |
| Source note | uspto-grants-2004_11 |