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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2415453Generated: November 3, 2026

Triethylamine → HCID 10473439, compound

https://huagongshe.com/reaction/2415453

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantEthyl AcetateHCID 8857—
ReactantHCID 69036512HCID 69036512—
CatalystBis(triphenylphosphine)palladiumHCID 10122028—
ProductHCID 10473439HCID 1047343925%

Reaction Steps

As described for example 20f, the title compound (10 mg, 25%) was prepared from a mixture of 2-(R)-{2-[5-(4-Fluoro-benzyloxy)-2-iodo-phenyl]-acetylamino}-propionamide (50 mg, 0.109 mmol), triethylamine (0.030 mL, 0.218 mmol), bis (triphenylphosphine) palladium II chloride (1.5 mg, 0.0022 mmol) in 1 mL ethyl acetate. MS: m/e=357.2 (M+H+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06818774B2
Source datasetuspto-grants-2004_11
ORD IDord-65544c9976a445d892f80542377efe56
Source noteuspto-grants-2004_11