Thionyl Chloride → HCID 12994203, compound

HRID 2415633Notes

Reaction equation

HRID 2415633 reaction equation
[C:1]([O:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]2[CH:16]=[CH:15][C:14]([C:17]([OH:19])=O)=[CH:13][CH:12]=2)=[CH:7][CH:6]=1)(=[O:3])[CH3:2].S(Cl)([Cl:22])=O>>[C:1]([O:4][C:5]1[CH:10]=[CH:9][C:8]([C:11]2[CH:16]=[CH:15][C:14]([C:17]([Cl:22])=[O:19])=[CH:13][CH:12]=2)=[CH:7][CH:6]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 6118364'-Acetoxy-biphenyl-4-carboxylic acid

Product 1

HCID 12994203HCID 12994203, compound

Conditions

Temperature
79 °C

Procedure

A reactor was charged with 59.8 g (233.4 mmol) of 4′-acetoxybiphenyl-4-carboxylic acid and 278 g (2.33 mol) of purified thionyl chloride, and a mixture was refluxed under heat (79° C.) for 4 hours.

Workup

  1. temperaturea mixture was refluxed

Sources & evidence

ORD record
ord-de614905dffc403a94108898429a627e
Source dataset
uspto-grants-2004_11
Patent number
US06821581B2

Reaction notes

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