Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4'-Acetoxy-biphenyl-4-carboxylic acid | HCID 611836 | — |
| Product | HCID 12994203 | HCID 12994203 | — |
Reaction Steps
A reactor was charged with 59.8 g (233.4 mmol) of 4′-acetoxybiphenyl-4-carboxylic acid and 278 g (2.33 mol) of purified thionyl chloride, and a mixture was refluxed under heat (79° C.) for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06821581B2 |
|---|
| Source dataset | uspto-grants-2004_11 |
|---|
| ORD ID | ord-de614905dffc403a94108898429a627e |
|---|
| Source note | uspto-grants-2004_11 |
|---|
