HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 69923056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 69922801 | HCID 69922801 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69923056 | HCID 69923056 | — |
Reaction Steps
A reactor was charged with 14 g (36 mmol) of (R)-1-methyloctyl-4′-acetoxybiphenyl-4-carboxylate and 150 ml of toluene, 5.7 g of a methanol solution containing 40% methylamine (73 mmol % of methylamine) was dropwise added, and a mixture was stirred at room temperature for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06821581B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-12e8a36f808141da88e11960e130f365 |
| Source note | uspto-grants-2004_11 |