HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(5-Methoxy-1,2-benzisoxazolyl)piperidine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Acetyl-4-(5-methoxy-1,2-benzisoxazolyl)piperidine | HCID 13076418 | — |
| Product | 4-(5-Methoxy-1,2-benzisoxazolyl)piperidine hydrochloride | HCID 13076425 | — |
Reaction Steps
0.07 mol of 1-acetyl-4-(5-methoxy-1,2-benzisoxazolyl)piperidine and 110 ml of 6N HCl is refluxed for 6 hours and stand at room temperature to precipitate large amount of white deposit, which is recrystallized in ethanol to obtain 4-(5-methoxy-1,2-benzisoxazolyl)piperidine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08653069B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-3a0678ad8b5646cebc387c8570d35e4f |
| Source note | uspto-grants-2014_02 |