HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 17937292, compound → HCID 17937358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 17937292 | HCID 17937292 | — |
| Reactant | 5-(3,5-Diethoxy-4-iodo-benzyl)-pyrimidine-2,4-diamine | HCID 22636919 | — |
| Reactant | 3,4-Dimethoxyphenylboric acid | HCID 22637025 | — |
| Product | HCID 17937358 | HCID 17937358 | — |
Reaction Steps
Starting from 5-(3,5-diethoxy-4-iodo-benzyl)-pyrimidine-2,4-diamine (example 1) (414 mg; 1.0 mmol) and 3,4-dimethoxy-phenyl-boric acid (363 mg; 2.0 mmol), 328 mg (77%) 5-(3,5-diethoxy-4-thiophen-3-yl-benzyl)-pyrimidine-2,4-diamine [sic] are obtained as a yellowish powder after recrystallization from methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06821980B1 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-8349e1831abd4f29a678e8cce91ce915 |
| Source note | uspto-grants-2004_11 |