HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 22636917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | 4-(2-Chloroacetyl) thiomorpholine | HCID 18918637 | — |
| Reactant | HCID 22636973 | HCID 22636973 | — |
| Product | HCID 22636917 | HCID 22636917 | — |
Reaction Steps
The 1-thiomorpholin-4-yl-2-(5-trimethylstannanyl-thiophen-2-ylmethoxy)-ethanone employed is prepared analogously to example (3a) (stage b)) starting from (5-trimethylstannanyl-thiophen-2-yl)-methanol (7.66 g; 27.67 mmol; described, in example (3a), stage a)), sodium iodide (4.07 g; 27.34 mmol) and 2-chloro-1-thiomorpholiri-4-yl-ethanone (5.92 g; 32.94 mmol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06821980B1 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-681e745c06394b75adb880faeba41a1c |
| Source note | uspto-grants-2004_11 |