Hydrochloric Acid → 4-(N,N-Dimethylcarbamimidoyl)benzoic acid hydrochloride

HRID 2416578Notes

Reaction equation

HRID 2416578 reaction equation
[CH3:1][N:2]([CH3:16])[C:3]([C:5]1[CH:15]=[CH:14][C:8]([C:9]([O:11]CC)=[O:10])=[CH:7][CH:6]=1)=[NH:4].[ClH:17]>>[ClH:17].[CH3:1][N:2]([CH3:16])[C:3]([C:5]1[CH:15]=[CH:14][C:8]([C:9]([OH:11])=[O:10])=[CH:7][CH:6]=1)=[NH:4]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 22631319ethyl 4-(N,N-dimethylamidino)benzoate

Product 1

HCID 534445094-(N,N-Dimethylcarbamimidoyl)benzoic acid hydrochloride

Procedure

Ethyl 4-(N,N-dimethylamidino)benzoate and 6 N hydrochloric acid were heated under reflux for 6 hours and then the solvent was evaporated to obtain the title compound.

Workup

  1. temperatureunder reflux for 6 hours
  2. customthe solvent was evaporated

Sources & evidence

ORD record
ord-99e6de9020d24f5e893ecb3c9fec73c1
Source dataset
uspto-grants-2004_11
Patent number
US06825181B1

Reaction notes

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