HCID 54434818, compound → HCID 22632123, compound

Participants

Reaction Steps

According to the procedure of Example 1(c), except substituting methyl (±)-8-[3-[(4-methoxy-2-pyridyl)amino]-1-propyloxy]-3-oxo-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate for the ethyl (±)-8-[3-(2-pyridylamino)-1-propyloxy]-3-oxo-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate, the title compound was prepared as an off-white solid: MS (ES) m/e 400.3 (M+H)+. Anal. Calcd for C21H25N3O5.0.75 H2O: C, 61.08; H, 6.47; N, 10.18. Found: C, 61.15; H, 6.20; N, 10.12.

Provenance & Evidence