HCID 54296195, compound → HCID 22632200, compound

Participants

Reaction Steps

According to the procedure of Example 1(c), except substituting methyl (±)-8-[3-(4-aminopyridin-2-ylamino)-1-propyloxy]-2-methyl-3-oxo-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate for the ethyl (±)-8-[3-[2-pyridylamino)-1-propyloxy]-3-oxo-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate, the title compound was prepared as a white solid: MS (ES) m/e 399 (M+H)+. Anal. Calcd for C21H26N4O4.1.5CF3CO2H.0.125H2O: C, 50.62: H, 4.91; N, 9.83. Found: C, 50.63; H 5.26; N, 9.90.

Provenance & Evidence