HCID 53957185, compound → HCID 22632202, compound

Participants

Reaction Steps

According to the procedure of Example 1(c), except substituting methyl (±)-3-oxo8-[3-[N-(pyridin-2-yl)-N-(tert-butoxycarbonyl)amino]-1-propyloxy]-2-(4-trifluoromethylbenzyl)-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate for the ethyl (±)-8-[3-(2-pyridylamino)-1-propyloxy]-3-oxo-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate, the title compound was prepared as an off-white solid: MS (ES) m/e 628.4 (M+H)+. Anal. Calcd for C33H36F3N3O6.0.5 H2O: C, 62.25; H, 5.86; N, 6.60. Found C, 62.01; H, 5.92; N, 6.81.

Provenance & Evidence