HCID 54434818, compound → HCID 22632139, compound

Participants

Reaction Steps

According to the procedure of Example 1(c) except substituting methyl (±)-2-(carboxymethyl)-3-oxo-8-[3-(pyridin-2-ylamino)-1-propyloxy]-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate for the ethyl (±)-8-[3-(2-pyridylamino)-1-propyloxy]-3-oxo-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate, the title compound (0.30 g, 56%) was prepared: MS (ES) m/e 428.4 (M+H)+. Anal. Calcd for C22H25N3O6.2 H2O: C, 57.01; H, 6.31; N, 9.07; Found: C, 57.27; H, 6.24; N, 8.86.

Provenance & Evidence