HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53957185, compound → HCID 57459730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53957185 | HCID 53957185 | — |
| Reactant | HCID 86591934 | HCID 86591934 | — |
| Product | HCID 57459730 | HCID 57459730 | 60% |
Reaction Steps
According to the procedure of Example 24(c) except substituting methyl (S)-3-oxo-8-[3-[N-(pyridin-2-yl)-N-(tert-butoxycarbonyl)amino]-1-propyloxy]-2-(4-trifluoromethylbenzyl)-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate for the methyl (±)-3-oxo-8-[3-[N-(pyridin-2-yl)-N-(tert-butoxycarbonyl)amino]-1-propyloxy]-2-(4-trifluoromethylbenzyl)-2,3,4,5-tetrahydro-1H-2-benzazepine-4-acetate, the title compound (0.8 g, 60%) was prepared: MS (ES) m/e 628.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825188B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-869a6d74e17b47afa6cc3c0b83d2b7a8 |
| Source note | uspto-grants-2004_11 |