HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22633010, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | Benzyloxyamine hydrochloride | HCID 102312 | — |
| Reactant | HCID 22632910 | HCID 22632910 | — |
| Product | HCID 22633010 | HCID 22633010 | 103.6% |
Reaction Steps
Using General Method 2, the reaction of carbonyldiimidazole (2.85 g, 17.6 mmol), 2-(2,4,5-trifluoro-anilino)-4,5-difluorobenzoic acid (Example T, 4.54 g, 14.7 mmol), O-benzylhydroxylamine hydrochloride (2.34 g, 14.7 mmol), and triethylamine (2.45 mL, 17.6 mmol) provided 6.22 g of the crude title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825199B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-b37ec7ebce4448308271d79ca3863139 |
| Source note | uspto-grants-2004_11 |