HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22632898, compound → HCID 22632881, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22632898 | HCID 22632898 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 22632881 | HCID 22632881 | 93.2% |
Reaction Steps
Using the General Method 6A, the reaction of 10% Pd/C (0.04 g) with 1-(3-methoxyphenyl)-6-fluoro-3-benzyloxy-7-pyrrolidin-1-yl-1H-quinazoline-2,4-dione (Example T-1, 0.12 g, 0.26 mmol) afforded 0.09 g of the title compound as a solid, mp 216-218° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825199B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-c8360e2abea5411fafa9d58c25edc13c |
| Source note | uspto-grants-2004_11 |