HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Mercaptophenol → Ethyl(3-chlorophenyl)[(4-hydroxyphenyl)sulfanyl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Mercaptophenol | HCID 240147 | — |
| Reactant | Ethyl 2-Bromo-2-(3-chlorophenyl)acetate | HCID 12717576 | — |
| Product | Ethyl(3-chlorophenyl)[(4-hydroxyphenyl)sulfanyl]acetate | HCID 131724674 | 82% |
Reaction Steps
Ethyl(3-chlorophenyl)[(4-hydroxyphenyl)sulfanyl]acetate was prepared according to the general method as outlined in example 1 (step 1), starting from ethyl bromo(3-chlorophenyl)acetate (6.16 g, 16.5 mmol) and 4-mercaptophenol (2.08 g, 16.5 mmol); 4.36 g clear oil. Yield 82%; MS: 321 (M−H)−
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825354B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-834dc981e2f34c8d860f0dfacb6cff05 |
| Source note | uspto-grants-2004_11 |