Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2417281Generated: November 2, 2026

1-Bromo-2-butyne → HCID 131724675, compound

https://huagongshe.com/reaction/2417281

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Bromo-2-butyneHCID 2756862—
ReactantHCID 90750084HCID 90750084—
ProductHCID 131724675HCID 13172467587%

Reaction Steps

Ethyl(2-methoxyphenyl){[4-(2-butynyloxy)phenyl]sulfanyl}acetate was prepared according to the general method as outlined in example 1 (step 2), starting from ethyl (2-methoxyphenyl)[(4-hydroxyphenyl)sulfanyl]acetate (3.2 g, 10 mmol) and 1-bromo-2-butyne (1.5 g, 11.2 mmol); 3.2 g clear oil. Yield 87%; MS(EI): 371 (M+H)+

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06825354B2
Source datasetuspto-grants-2004_11
ORD IDord-95a8241e97fb40fe98148373f1f00d34
Source noteuspto-grants-2004_11