HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-butyne → HCID 131724675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-butyne | HCID 2756862 | — |
| Reactant | HCID 90750084 | HCID 90750084 | — |
| Product | HCID 131724675 | HCID 131724675 | 87% |
Reaction Steps
Ethyl(2-methoxyphenyl){[4-(2-butynyloxy)phenyl]sulfanyl}acetate was prepared according to the general method as outlined in example 1 (step 2), starting from ethyl (2-methoxyphenyl)[(4-hydroxyphenyl)sulfanyl]acetate (3.2 g, 10 mmol) and 1-bromo-2-butyne (1.5 g, 11.2 mmol); 3.2 g clear oil. Yield 87%; MS(EI): 371 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825354B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-95a8241e97fb40fe98148373f1f00d34 |
| Source note | uspto-grants-2004_11 |