HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 11750539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 11360973 | HCID 11360973 | — |
| Product | HCID 11750539 | HCID 11750539 | 89% |
Reaction Steps
Ethyl(1-acetyl-4-piperidinyl){[4-(2-butynyloxy)phenyl]sulfonyl}acetate was prepared according to the general method as outlined in example 116 (step 1), starting from ethyl{[4-(2-butynyloxy)phenyl]sulfonyl}(4-piperidinyl)acetate (1.5 g, 3.61 mmol) and acetyl chloride (0.26 ml, 3.61 mmol); yellow oil (1.35 g). Yield 89%; MS: 422 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825354B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-9509ea3e4fce4760bfc5d1bea177df54 |
| Source note | uspto-grants-2004_11 |