HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boronic Acid → 2-Propyloxy-5,6,7,8-tetrahydro-5,5,8,8-tetra-methylnaphthylboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boronic Acid | HCID 61668 | — |
| Reactant | 2-Bromo-3-propoxy-5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene | HCID 22252753 | — |
| Product | 2-Propyloxy-5,6,7,8-tetrahydro-5,5,8,8-tetra-methylnaphthylboronic acid | HCID 22634657 | — |
Reaction Steps
In a similar manner to Example 3(a), by reaction of 8 g (24.6 mmol) of 3-bromo-2-propyloxy-5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene, 5.7 g (80%) of the expected boronic acid are obtained, with a melting point of 138-9° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06825360B1 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-790107d14227438cb80bfc7d54f4a4c2 |
| Source note | uspto-grants-2004_11 |