HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 69817674, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10113837 | HCID 10113837 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69817674 | HCID 69817674 | — |
Reaction Steps
To a solution of 10% hydrogen chloride in methanol was added N-[4-[(2S)-3-hydroxy-2-[[(2S)-2-hydroxy-3-phenoxypropyl]amino)propyl]phenyl]-N′-phenylurea (70 mg) and stirred for 15 minutes. The reaction mixture was concentrated and followed by recrystallization from ethanol to give N-[4-[(2S)-3-hydroxy-2-([(2S)-2-hydroxy-3-phenoxypropyl]amino]propyl]phenyl]-N′-phenylurea hydrochloride (38 mg) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06826033B2 |
| Source dataset | uspto-grants-2004_11 |
| ORD ID | ord-8c893b9eca7e476abcfcfae418edf41d |
| Source note | uspto-grants-2004_11 |