Triethylamine → HCID 86589873, compound

Participants

Reaction Steps

4.2 g (13.1 mmol) of ethyl (4-bromo-2-nitrobenzyl)aminoacetate was dissolved in 30 ml of dichloromethane. 2.2 ml (17.7 mmol) of 4-chlorobenzoyl chloride and 2.9 ml (19.6 mmol) of triethylamine were added to the obtained solution, and they were stirred overnight. After the treatment with dichloromethane as the extracting solvent by an ordinary method, the obtained crude product was purified by the silica gel column chromatography to obtain the crude product.

Provenance & Evidence