Triethylamine → HCID 86589877, compound

Participants

Reaction Steps

1.15 g (3.95 mmol) of ethyl (5-fluoro-2-nitrobenzyl)aminoacetate was dissolved in 20 ml of dichloromethane. 0.61 ml (4.7 mmol) of 4-chlorobenzoyl chloride and 0.82 ml (5.9 mmol) of triethylamine were added to the obtained solution, and they were stirred at room temperature for 2 hours. After the treatment with dichloromethane as the extracting solvent by an ordinary method, the crude product was obtained.

Provenance & Evidence