HRID2417574
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
0.1 Mole of alpha-chlorolauric acid prepared in the foregoing manner was admixed with 500 mls. water and 0.4 moles of KOH in a suitable reaction vessel and stirred overnight at a temperature of 98°-100° C. The reaction mixture was poured into a separatory funnel, to which was added hydrochloric acid (40 ml. conc. HCl in 200 ml. H2O). The mixture was extracted with chloroform. The chloroform layer was removed and the CHCl3 evaporated to yield alpha-hydroxylauric acid.
WORKUP
后处理
- additionThe reaction mixture was poured into a separatory funnel, to which
- extractionThe mixture was extracted with chloroform
- customThe chloroform layer was removed
- customthe CHCl3 evaporated