HCID 178430796, compound → HCID 178460861, compound
Reaction equation
CC1(C)[NH:6][CH:5]([PH:7](=[O:9])[OH:8])[C:4]([CH3:11])([CH3:10])[S:3]1>O>[NH2:6][CH:5]([PH:7](=[O:8])[OH:9])[C:4]([SH:3])([CH3:11])[CH3:10]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 0 °C
Procedure
0.5 g of DL-(2,2,5,5-tetramethyl-4-thiazolidinyl)phosphinic acid (prepared as described in Example 2) was dissolved in boiling water and the solution was concentrated by boiling. The solution was cooled to 0° C. and the white crystalline solid was collected. There was obtained 0.15 g of DL-(1-amino-2-mercapto-2-methylpropyl)phosphinic acid of melting point 205°-207° C. (decomposition).
Workup
- concentrationthe solution was concentrated
- customthe white crystalline solid was collected
Sources & evidence
- ORD record
- ord-af3f33cfb11446fdb8172d97996cc14e
- Source dataset
- uspto-grants-1984_09
- Patent number
- US04469686
Reaction notes
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