HCID 178430796, compound → HCID 178460861, compound

Participants

Reaction Conditions

Reaction Steps

0.5 g of DL-(2,2,5,5-tetramethyl-4-thiazolidinyl)phosphinic acid (prepared as described in Example 2) was dissolved in boiling water and the solution was concentrated by boiling. The solution was cooled to 0° C. and the white crystalline solid was collected. There was obtained 0.15 g of DL-(1-amino-2-mercapto-2-methylpropyl)phosphinic acid of melting point 205°-207° C. (decomposition).

Provenance & Evidence