HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 4-Acetoxy-5-[4-(4-trifluoromethylphenoxy)phenoxy]-2-hexanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Hexanone, 4-hydroxy-5-[4-[4-(trifluoromethyl)phenoxy]phenoxy]- | HCID 20278399 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Acetoxy-5-[4-(4-trifluoromethylphenoxy)phenoxy]-2-hexanone | HCID 20447578 | — |
Reaction Steps
To 4-hydroxy-5-[4-(4-trifluoromethylphenoxy)phenoxy]-2-hexanone (3.5 mmol) and pyridine (3.5 mmol) in benzene (20 ml) is added acetyl chloride (4.0 mmol). The mixture is stirred at RT overnight. The reaction mixture is diluted with benzene, washed with water, dried and the solvent is removed in vacuo to give 4-acetoxy-5-[4-(4-trifluoromethylphenoxy)phenoxy]-2-hexanone (cpd. 10, Table B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04469872 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-7d1e9c4b207346218f70982fb44a6b24 |
| Source note | uspto-grants-1984_09 |