HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 54509253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4372-17-2 | HCID 231457 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 54509253 | HCID 54509253 | — |
Reaction Steps
To dry ethyl ether (55.0 ml) under nitrogen was added ethyl 2-(2-butyl)malonic acid (55.0 g, 0.29 mole). Thionyl chloride (32.0 ml, 52.5 g, 0.44 mole) was added dropwise with stirring. The solution was heated to 50° C. for 2 hours under nitrogen, at which time no further HCl was evolved.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04470421 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-b683ba0db4b3439f84b7b2a075f4f89c |
| Source note | uspto-grants-1984_09 |