Acetic Anhydride → HCID 54503292, compound

Participants

Reaction Steps

To a solution of 1.36 g of 4-aminophenyl 4-O-(β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside in 7 ml of water was added 0.463 g of acetic anhydride. The solution was shaken for 5 minutes then taken to dryness. The resulting glass was triturated with ethyl acetate and the solid collected, giving 1.49 g. of the desired intermediate as a white glass.

Provenance & Evidence