HuagongsheHuagongshe Chemistry Print Report · For research reference only
Monobenzone → 1-(Benzyloxy)-4-[(6-bromohexyl)oxy]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Monobenzone | HCID 7638 | — |
| Reactant | 1,6-Dibromohexane | HCID 12368 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1-(Benzyloxy)-4-[(6-bromohexyl)oxy]benzene | HCID 13450883 | — |
Reaction Steps
4-Benzyloxyphenol and 1,6-dibromohexane were reacted using conditions reported in Example 15. The reaction time was 4 days and the extraction solvent used was toluene. The crude product was crystallized from hexane to give 1-benzyloxy-4-(6-bromohexyloxy)benzene, mp 72°-3°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04471116 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-a6cd268966a243e99939ef739c4038d4 |
| Source note | uspto-grants-1984_09 |