HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → 1-Benzyloxy-4-[5-(1-methylethyl)aminopentoxy]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 1-(Benzyloxy)-4-[(5-bromopentyl)oxy]benzene | HCID 13219124 | — |
| Product | 1-Benzyloxy-4-[5-(1-methylethyl)aminopentoxy]benzene | HCID 20446946 | — |
Reaction Steps
As described in Example 19, 1-benzyloxy-4-(5-bromopentoxy)benzene was reacted with isopropylamine at 100° (12 hours; 150 psi) to give 1-benzyloxy-4-[5-(1-methylethyl)aminopentoxy]benzene. The distilled product was 95.2% pure by gas chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04471116 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-cd98b437db8c49509a7dc3fa2f4ac29e |
| Source note | uspto-grants-1984_09 |