HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → 1-Benzyloxy-4-[6-(1-methylethyl)aminohexyloxy]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | 1-(Benzyloxy)-4-[(6-bromohexyl)oxy]benzene | HCID 13450883 | — |
| Product | 1-Benzyloxy-4-[6-(1-methylethyl)aminohexyloxy]benzene | HCID 13338481 | — |
Reaction Steps
As described in Example 19, 1-benzyloxy-4-(6-bromohexyloxy)benzene was reacted with isopropylamine at 100° (12 hours; 500 psi) to give 1-benzyloxy-4-[6-(1-methylethyl)aminohexyloxy]benzene. The crude oil was crystallized from pentane yielding the purified product, mp 47°-49°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04471116 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-a12716c74ce84a73acd2f1c10e98f378 |
| Source note | uspto-grants-1984_09 |