Allyl bromide → HCID 20446065, compound

HRID 2418274Notes

Reaction equation

HRID 2418274 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH2:9][C:10]([CH3:20])([CH2:17][CH:18]=[CH2:19])[CH2:11][N:12]1[CH2:16][CH2:15][CH2:14][CH2:13]1.[CH2:21]([Br:24])[CH:22]=[CH2:23]>C(OCC)(=O)C>[Br-:24].[CH2:23]([N+:12]1([CH2:11][C:10]([CH3:20])([CH2:17][CH:18]=[CH2:19])[CH2:9][C:3]2[CH:4]=[CH:5][C:6]([Cl:8])=[CH:7][C:2]=2[Cl:1])[CH2:16][CH2:15][CH2:14][CH2:13]1)[CH:22]=[CH2:21]

Participants

4

Reactant 2

HCID 7841Allyl bromideHCID 13189987HCID 13189987, compound

Product 1

HCID 20446065HCID 20446065, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

A solution of 40 g of (X) and 31.5 g of allyl bromide in 300 ml of ethyl acetate was refluxed for 5 hours. The precipitated product was filtered off under suction, washed with ethyl acetate and dried under reduced pressure. Yield: 15 g; melting point: 174° C. (compound No. 56).

Workup

  1. filtrationThe precipitated product was filtered off under suction
  2. washwashed with ethyl acetate
  3. customdried under reduced pressure

Sources & evidence

ORD record
ord-39b2470ab5a3452285efa4f405fe1f33
Source dataset
uspto-grants-1984_09
Patent number
US04472412

Reaction notes

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