Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 13189988 | HCID 13189988 | — |
| Product | HCID 13189989 | HCID 13189989 | 78.8% |
Reaction Steps
332 g of (XX) were added dropwise to 148 g of thionyl chloride, and the mixture was stirred for 14 hours at room temperature and for 2 hours at 140° C. Distillation gave 278 g of (XXI) of boiling point 142°-145° C./0.1 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04472412 |
|---|
| Source dataset | uspto-grants-1984_09 |
|---|
| ORD ID | ord-b5423466a6314bcca98fe7e4f4bc96ca |
|---|
| Source note | uspto-grants-1984_09 |
|---|
