HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 86739638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | HCID 13142003 | HCID 13142003 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86739638 | HCID 86739638 | — |
Reaction Steps
A solution of 34.8 g of (XXII) and 36.3 g of allyl bromide in 250 ml of ethyl acetate was refluxed for 5 hours. The product, which was obtained as an oil, was washed several times with ethyl acetate and then freed from residual solvent under reduced pressure. Yield: 32 g of a yellowish brown resin (compound No. 60).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472412 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-cb0adc6266a84de29b08646488b2c08f |
| Source note | uspto-grants-1984_09 |