Allyl bromide → HCID 86739638, compound

HRID 2418280Notes

Reaction equation

HRID 2418280 reaction equation
[CH2:1]([CH:5]([CH2:12][C:13]1[CH:18]=[CH:17][C:16]([Cl:19])=[C:15]([Cl:20])[C:14]=1[Cl:21])[CH2:6][N:7]1[CH2:11][CH2:10][CH2:9][CH2:8]1)[CH2:2][CH2:3][CH3:4].[CH2:22]([Br:25])[CH:23]=[CH2:24]>C(OCC)(=O)C>[Br-:25].[CH2:24]([N+:7]1([CH2:6][CH:5]([CH2:1][CH2:2][CH2:3][CH3:4])[CH2:12][C:13]2[CH:18]=[CH:17][C:16]([Cl:19])=[C:15]([Cl:20])[C:14]=2[Cl:21])[CH2:11][CH2:10][CH2:9][CH2:8]1)[CH:23]=[CH2:22]

Participants

4

Reactant 2

HCID 7841Allyl bromideHCID 13142003HCID 13142003, compound

Product 1

HCID 86739638HCID 86739638, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

A solution of 34.8 g of (XXII) and 36.3 g of allyl bromide in 250 ml of ethyl acetate was refluxed for 5 hours. The product, which was obtained as an oil, was washed several times with ethyl acetate and then freed from residual solvent under reduced pressure. Yield: 32 g of a yellowish brown resin (compound No. 60).

Workup

  1. customThe product, which was obtained as an oil
  2. washwas washed several times with ethyl acetate

Sources & evidence

ORD record
ord-cb0adc6266a84de29b08646488b2c08f
Source dataset
uspto-grants-1984_09
Patent number
US04472412

Reaction notes

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