HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → Acetanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 54151966 | HCID 54151966 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Acetanilide | HCID 904 | — |
Reaction Steps
5.4 grams (0.020 moles) of 2-thenoylmercaptopropionylglycine were added to 50 ml of tetrahydrofurane. The temperature of the resulting mixture was brought to 0° C., then a solution of ethylchloroformate (2.2 grams; 0.020 moles) in 10 ml of anhydrous CH2Cl2 was slowly added. To the resulting solution, the following solution was slowly added:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472424 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-f00f7553e5424222a6e1c4fcaf05908b |
| Source note | uspto-grants-1984_09 |