HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 54118377, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Butenoyl chloride | HCID 79080 | — |
| Reactant | HCID 22827697 | HCID 22827697 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54118377 | HCID 54118377 | — |
Reaction Steps
To 6.39 g (0.03 mol) of N-(2,4-dimethylthien-3-yl-alanine-methylester, 4.15 g (0.03 mol) of K2CO3, 10 ml of water and 100 ml of dichloromethane are added without cooling 3.14 g (0.03 mol) 2-butenoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472425 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-dc1e4e81ad2c41a6aba6eb983deaacf5 |
| Source note | uspto-grants-1984_09 |