Toluene → HCID 20446128, compound

Participants

Reaction Steps

0.73 g (0.03 mol) NaH and 7.95 (0.03 mol) methyl 2-(2,4-dimethylthien-3-yl)-2-(methoxyacetyl)-hydrazinecarboxylate in 100 ml dry toluene are heated under reflux for 3 hours. The reaction mixture is then, together with 9.52 g (0.067 mol) CH3J, transferred into a sealed cylinder and heated 20 hours at 110°. The mixture is, after cooling, diluted with diethylether, washed with water, dried and evaporated to yield the title compound.

Provenance & Evidence