HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → N-(2,4-Dimethylthiophen-3-yl)-2-methoxyacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methoxyacetyl chloride | HCID 96623 | — |
| Reactant | 2,4-Dimethylthiophen-3-amine | HCID 13341198 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-(2,4-Dimethylthiophen-3-yl)-2-methoxyacetamide | HCID 13341230 | — |
Reaction Steps
To 12.7 g (0.1 mol) of 2,4-dimethyl-3-aminothiophene, 13.84 g (0.1 mol) of K2CO3, 50 ml of water and 160 ml of methylene chloride are added without cooling 10.8 g (0.1 mol) of methoxyacetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472425 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-043384c35a7241f89787a6dc3bc4aabb |
| Source note | uspto-grants-1984_09 |