HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzoyl isocyanate → HCID 13041497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzoyl isocyanate | HCID 12259962 | — |
| Reactant | HCID 13041496 | HCID 13041496 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 13041497 | HCID 13041497 | — |
Reaction Steps
6.54 g (0.03 Mol) of 4-(2,2-dichlorcyclopropyloxy)-aniline, dissolved in 50 ml dry tetrahydrofuran, are added dropwise with 4.84 g (0.03 Mol) of 2-methylbenzoyl-isocyanate, with stirring. The temperature increases mildly therewith. After cooling, the product is precipitated with pentane, withdrawn by suction, after-washed with pentane and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472434 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-9f743dcb08734b869fc4bd3da213e0b5 |
| Source note | uspto-grants-1984_09 |