HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenol → 2-[2-Nitro-3-(4-chlorophenoxy)phenyl]acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 2-(3-chloro-2-nitrophenyl)acetate | HCID 20446267 | — |
| Product | 2-[2-Nitro-3-(4-chlorophenoxy)phenyl]acetic acid | HCID 20446193 | 54.6% |
Reaction Steps
A mixture of ethyl 2-(2-nitro-3-chlorophenyl)acetate (10 g.), 4-chlorophenol (7.8 g.), anhydrous potassium carbonate (8.5 g.) and cupric oxide (3 g.) was treated in a similar manner to the above Preparations to give 2-[2-nitro-3-(4-chlorophenoxy)phenyl]acetic acid (6.9 g.). mp 167° to 170° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04472433 |
| Source dataset | uspto-grants-1984_09 |
| ORD ID | ord-a4144ec4f83747db8147823d1b4faf82 |
| Source note | uspto-grants-1984_09 |